Emalabhorethri okuhlola ezemvelo asebenza ngama-Volatile Organic Compounds (VOCs) asezingeni eliphansi ngokusebenzisa i-Purge-and-Trap GC-MS (njenge-EPA Methods 524.2, 524.3, 624.1, kanye ne-8260D), ukungcola kwe-method blank kuyimbangela eyinhloko yokwehluleka kwama-Quality Control (QC) batches. Ama-vial angu-40 mL VOA (Volatile Organic Analysis) angabizi noma angagunyaziwe avame ukukhipha i-benzene, i-toluene, ama-xylenes (BTEX), noma ama-phthalate plasticizers, ephakamisa imikhawulo yokutholwa kwendlela futhi ebangela ukuphindwa kwe-batch.
Okubalulekile Okutholakele
- Imbangela Eyinhloko Yokwehluleka Kwe-QC Blank:
- Izindinganiso Ze-EPA Protocol: I-EPA Protocol B
- Isixazululo Esiphelele: ama-vial angu-40 mL VOA ahlanzekile agunyaziwe, ama-septa angu-0.125" (3.18 mm) e-PTFE/Silicone amsulwa
Imithombo Evamile Yama-Artifact Angemuva Kuma-Vial angu-40 mL VOA
I-Low-Grade Liner/Ukupakisha ➔ Ukukhishwa kwe-Plasticizer ne-Hydrocarbon ➔ Ukuhlanganiswa kwe-Purge-and-Trap ➔ Ama-ion aphezulu e-m/z 77, 91, 149 ➔ Ukwehluleka kwe-QC Blank kanye nokuphinda kuthathwe amasampula yikhasimende
- Ukungcola kwe-Phthalate (149):
- Ukugcinwa kwe-Septum Solvent (77, 91, 106):
- Ubukhulu be-Septum obungafanele kanye nokukhipha umgogodla:0.125"
Ukuqhathanisa kwekhwalithi: Amaviyela ajwayelekile vs. Amaviyela e-CHANCEPRO Certified EPA VOA
Ipharamitha | Amaviyela ajwayelekile / anezindleko eziphansi angu-40 mL | Amaviyela e-CHANCEPRO Certified Pre-Cleaned EPA VOA |
Izinga lokuhlanza | Ukuhlanza okuyisisekelo / okungaqinisekisiwe | I-EPA Protocol B (ukugezwa nge-asidi, ukugezwa nge-DI, ukubhaka nge-400°C) |
Ukucaciswa Kwe-Septum | i-silicone yezohwebo engu-0.060" – 0.090" | I-0.125" (3.18 mm) ye-High-Resilience Medical Grade PTFE/Silicone |
Ukunamathela kwe-Liner | Ukunamathiselwa nge-glue (ingozi ye-organic solvent) | Ukucindezelwa kwe-Bi-layer okungenayo i-Glue 100%/Sonic Fit |
Ukulandelela i-VOC Background | Imvamisa iqukethe i-BTEX/Phthalates | < Umkhawulo wokutholwa kwendlela (MDL < 0.05 ) |
Imibhalo | Incwadi ejwayelekile yokuthobela | I-Certificate of Analysis (CoA) ye-GC-MS & TOC eqondene neqoqo |
Indawo yokupakisha | Ibhokisi elijwayelekile le-warehouse | Iphakethe le-Cleanroom elivalwe nge-vacuum le-Class 10,000 |
Izinqubo ezi-4 zokuvimbela imiphumela engamanga emaqoqweni e-Trace VOC
- Qinisekisa ama-CoA aqondene neqoqo ngaphambi kokusebenzisa:
- Umthetho wokuthatha isampula ongenayo i-Headspace:
- Sebenzisa ama-Liner ama-PTFE Amsulwa angu-0.125" (3.18 mm):
- Faka Ama-Blank Ahlukile Okuvakasha Nensimu:
Izixazululo ze-CHANCEPRO eziqinisekisiwe ze-EPA/VOA Sampling
Kuklanyelwe ukuhlangabezana nezidingo zokuthobela imithetho zeziphathimandla zikamasipala ezinomthamo ophezulu, amalabhorethri ezemvelo ezohwebo, kanye nezicelo zokuhlola ezemvelo:
- Amabhodlela e-VOA aqinisekisiwe angu-40 mL e-Borosilicate acwebile noma ansundu (ukuqedwa kwe-24-400):
- Ama-Septa anzima angu-0.125" e-PTFE/Silicone:
- Imibhalo eqondene neqoqo: ukungenelela kwangemuva okungaziro